KMID : 1024519970060040385
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Journal of the Environmental Sciences 1997 Volume.6 No. 4 p.385 ~ p.389
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Multi-Pesticide Residue Method for Organopesticide Analysis
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Kim Woo-Seong
Lee Bong-Hun Bahn Kyeong-Nyeo Jung Sung-Ug Park Heung-Jai
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Abstract
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Pesticide residues were extracted with 70% acetone and transferred to dichloromethane. Extracts were applied to open-column chromatography with florisil and alumina-N. The final extract was analyzed by gas chromatography with electron-capture detector(GC /ECD) and nitrogen-phosphorus detector(GC/NPD). Recoveries of the 17 organochlorine pegticides were ranged from 60.8 to 84.9% and those of 15 organophosphate pesticides, from 70.5% to 100.0%(except phosmet and azlnphos-methyls. The minimum detectable levels of this analytical method were low(0.021-0.058mg/kg).
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KEYWORD
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Organochlorine and organophosphate pesticide, florisil, alumina-N, gas chromatography, GC/ECD, GC/NPD
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